ABSTRACT Title of dissertation: Wave Chaos Studies and The Realization of Photonic Topological Insulators Bo Xiao, Doctor of Philosophy, 2022 Dissertation directed by: Professor Steven Anlage Department of Electrical and Computer Engineering Wave propagation in various complex media is an interesting and practical field that has a huge impact in our daily life. Two common types of wave prop- agation are examined in this thesis: electromagnetic wave propagation in complex wave chaotic enclosures, where I studied its statistical properties and explored time- domain pulse focusing, and unidirectional edge modes propagating in a reciprocal photonic topological insulator waveguide. Several theories, e.g. the Random Matrix Theory and the Random Coupling Model, have been developed and validated in experiments to understand the statis- tical properties of the electromagnetic waves inside wave chaotic enclosures. This thesis extends the subject from a single cavity to a network of coupled cavities by creating an innovative experimental setup that scales down complex structures, which would otherwise be too large and cumbersome to study, to a miniature version that retains its original electromagnetic properties. The process involves shrinking down the metal cavity in size by a factor of 20, increasing the electromagnetic wave frequency by the same factor and cooling down the cavity by a dilution refrigera- tor to reduce its ohmic loss. This experimental setup is validated by comparison with results from a full-scale setup with a single cavity and it is then extended for multiple coupled cavities. In the time domain, I utilized the time-reversal mirror technique to focus electromagnetic waves at an arbitrary location inside a wave chaotic enclosure by injecting a numerically calculated wave excitation signal. I used a semi-classical ray algorithm to calculate the signal that would be received at a transceiver port resulting from the injection of a short pulse at the desired target location. The time-reversed version of this signal is then injected into the transceiver port and an approximate reconstruction of the short pulse is observed at the target port. Photonic topological insulators are an interesting class of materials whose pho- tonic band structure can have a bandgap in the bulk while supporting topologically protected unidirectional edge modes. This thesis presents a rotating magnetic dipole antenna, composed of two perpendicularly oriented coils fed with variable phase dif- ference, that can efficiently excite the unidirectional topologically protected surface waves in the bianisotropic metawaveguide (BMW) structure recently realized by Ma, et al., despite the fact that the BMW medium does not break time-reversal invariance. In addition to achieving high directivity, the antenna can be tuned con- tinuously to excite reflectionless edge modes to the two opposite directions with various amplitude ratios. Overall, this thesis establishes the foundation for further studies of the uni- versal statistical properties of wave chaotic enclosures, and tested the limits of its deterministic properties defined by the cavity geometry. It also demonstrated in experiment the excitation of a unidirectional edge mode in a Bianisotropic Meta- waveguide, allowing for novel applications in the field of communications, for exam- ple phased array antennas. Wave Chaos Studies and The Realization of Photonic Topological Insulators by Bo Xiao Dissertation submitted to the Faculty of the Graduate School of the University of Maryland, College Park in partial fulfillment of the requirements for the degree of Doctor of Philosophy 2022 Advisory Committee: Professor Steven Anlage, Chair/Advisor Professor Thomas Antonsen Professor Thomas Murphy Professor Neil Goldsman Professor Yanne Chembo Professor John Cumings, Dean’s Representative c© Copyright by Bo Xiao 2022 Acknowledgments For the work on testing the Random Coupling Model predictions in scaled- down cavities (Chapter 2 - 5), we acknowledge the assistance of Bisrat Addissie. This work was supported by ONR under Grant No. N000141512134, AFOSR COE Grant FA9550-15-1-0171 and ONR DURIP grant N000141410772, and the Maryland Center for Nanophysics and Advanced Materials. For the work on focusing waves at arbitrary location in a ray-chaotic enclosure using time-reversed synthetic sonas (Chapter 6), we thank the group of A. Richter (Uni. Darmstadt, Germany) for graciously loaning the cut-circle billiard, H.J. Paik and M. V. Moody for use of the pulsed tube refrigerator, Martin Sieber for comments on improving the short orbit calculation algorithm, and the High-Performance Com- puting Cluster at UMCP for use of the Deepthought cluster. This work is funded by the ONR under Grants No. N00014130474 and N000141512134, and the Center for Nanophysics and Advanced Materials (CNAM). For the work on exciting reflectionless unidirectional edge modes in a photonic topological insulator medium (Chapter 7), the work was supported by ONR under Grant No. N000141512134, AFOSR COE Grant FA9550-15-1-0171 and the National Science Foundation (NSF) under Grants No. DMR-1120923, No. PHY-1415547 and No. ECCS-1158644. ii Table of Contents List of Tables vi List of Figures vii List of Abbreviations xv 1 Introduction and Overview 1 1.1 Background . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2 1.2 Thesis Overview . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3 1.3 Ray-chaotic Cavities . . . . . . . . . . . . . . . . . . . . . . . . . . . 5 1.4 Random Matrix Theory . . . . . . . . . . . . . . . . . . . . . . . . . 7 1.4.1 Random Matrices . . . . . . . . . . . . . . . . . . . . . . . . . 7 1.4.2 Normalized Spacings Between The Nearest Eigenfrequencies . 8 1.5 Random Coupling Model . . . . . . . . . . . . . . . . . . . . . . . . . 9 1.5.1 S-parameters & Z-parameters . . . . . . . . . . . . . . . . . . 11 1.5.2 Normalized Impedance . . . . . . . . . . . . . . . . . . . . . . 12 1.5.3 Loss Parameter α . . . . . . . . . . . . . . . . . . . . . . . . . 13 1.5.4 Extensions of RCM . . . . . . . . . . . . . . . . . . . . . . . . 14 2 Testing The Random Coupling Model Predictions in a Scaled-Down Cavity With Remote Injection Setup 16 2.1 The Need For Scaled Cavities . . . . . . . . . . . . . . . . . . . . . . 18 2.2 Scaling of The Cavity . . . . . . . . . . . . . . . . . . . . . . . . . . . 20 2.2.1 Frequency Scaling . . . . . . . . . . . . . . . . . . . . . . . . . 20 2.2.2 Cavity Wall Conductivity Scaling . . . . . . . . . . . . . . . . 21 2.2.3 Scaling Limits . . . . . . . . . . . . . . . . . . . . . . . . . . . 26 2.3 Experimental Setup . . . . . . . . . . . . . . . . . . . . . . . . . . . . 26 2.3.1 VNA & Extenders . . . . . . . . . . . . . . . . . . . . . . . . 28 2.3.2 Cryostat . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 30 2.3.3 Free-space Propagation Path . . . . . . . . . . . . . . . . . . . 33 2.3.4 Mode Stirrer . . . . . . . . . . . . . . . . . . . . . . . . . . . . 36 2.4 Testing Experiments . . . . . . . . . . . . . . . . . . . . . . . . . . . 40 iii 2.4.1 Overall Plan . . . . . . . . . . . . . . . . . . . . . . . . . . . . 40 2.4.2 Free-space Propagation Path Measurement . . . . . . . . . . . 42 2.4.3 Collecting an Ensemble of Cavity Data . . . . . . . . . . . . . 42 2.4.4 Direct Injection . . . . . . . . . . . . . . . . . . . . . . . . . . 45 2.4.5 Remote Injection . . . . . . . . . . . . . . . . . . . . . . . . . 48 2.4.6 Extension to Multiple Connected Cavities . . . . . . . . . . . 48 2.4.7 Further Studies . . . . . . . . . . . . . . . . . . . . . . . . . . 50 3 Introducing Radiation Efficiency to the Random Coupling Model 54 3.1 Radiation Efficiency η and RCM With Lossy Ports . . . . . . . . . . 55 3.1.1 Zrad, Zant, Zcav and Zavg . . . . . . . . . . . . . . . . . . . . . 56 3.1.2 Radiation Efficiency η in One-port Systems . . . . . . . . . . 58 3.1.3 Radiation Efficiency η in Multi-port System . . . . . . . . . . 61 3.1.4 Scaling Relation Between α and η . . . . . . . . . . . . . . . . 61 3.2 Applying Radiation Efficiency η to Experimental Data . . . . . . . . 64 3.2.1 Calculating Loss Parameter Through Time-domain Energy Decay Time τ . . . . . . . . . . . . . . . . . . . . . . . . . . . 66 3.2.2 Fitting Radiation Efficiency η . . . . . . . . . . . . . . . . . . 67 3.2.3 η’s Independence From Cavity’s α . . . . . . . . . . . . . . . 70 3.2.4 Apply η to Experimental Data . . . . . . . . . . . . . . . . . 71 4 Single Scaled Cavity Experiment 74 4.1 Full-Scale Cavity Analysis . . . . . . . . . . . . . . . . . . . . . . . . 75 4.1.1 Frequency Dependent Loss Parameter . . . . . . . . . . . . . . 76 4.1.2 Fitting Error . . . . . . . . . . . . . . . . . . . . . . . . . . . 77 4.2 Miniature Cavity Analysis . . . . . . . . . . . . . . . . . . . . . . . . 79 4.2.1 Frequency Dependency of η and α . . . . . . . . . . . . . . . . 80 4.3 Comparison Between Full-Scale and Miniature Cavity . . . . . . . . . 82 4.3.1 Full-Scale Cavity with 1/4 absorber for N = 1 Frequency Segment . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 83 4.3.2 Full-Scale Cavity with 1/4 absorber for N = 10 Frequency Segments . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 84 4.4 α Range Limitation . . . . . . . . . . . . . . . . . . . . . . . . . . . . 86 4.4.1 Difference in Re[ξ11] and Re[ξ22] . . . . . . . . . . . . . . . . . 86 4.4.2 Difference in Re[ξ12], Re[ξ21] and Im[ξ12], Im[ξ21] . . . . . . . . 87 5 Multiple Scaled Cavity Experiment 91 5.1 Experimental Design . . . . . . . . . . . . . . . . . . . . . . . . . . . 92 5.1.1 Design considerations . . . . . . . . . . . . . . . . . . . . . . . 93 5.1.1.1 Cost efficient construction . . . . . . . . . . . . . . . 93 5.1.1.2 Efficient use of space and material . . . . . . . . . . 93 5.1.1.3 Flexible configuration . . . . . . . . . . . . . . . . . 100 5.1.1.4 Perturbers . . . . . . . . . . . . . . . . . . . . . . . . 103 5.1.1.5 Antenna and lens alignment . . . . . . . . . . . . . . 103 5.1.2 Assembled setup . . . . . . . . . . . . . . . . . . . . . . . . . 107 iv 5.2 Lessons Learned . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 108 5.2.1 Design assistance tools . . . . . . . . . . . . . . . . . . . . . . 110 5.2.1.1 CST modeling tool . . . . . . . . . . . . . . . . . . . 110 5.2.1.2 3D printed models . . . . . . . . . . . . . . . . . . . 112 5.2.2 Methods to Construct a Metal Box . . . . . . . . . . . . . . . 112 5.2.3 External vendors . . . . . . . . . . . . . . . . . . . . . . . . . 115 5.3 Experimental Results . . . . . . . . . . . . . . . . . . . . . . . . . . . 116 6 Focusing Waves at Arbitrary Locations in a Ray-Chaotic Enclosure Using Time-Reversed Synthetic Sonas 119 6.1 Introduction . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 120 6.2 Experiment . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 124 6.2.1 Calculation of Synthetic Sona . . . . . . . . . . . . . . . . . . 124 6.2.2 Experimental Setup . . . . . . . . . . . . . . . . . . . . . . . . 125 6.2.3 Frequency Domain Experiment . . . . . . . . . . . . . . . . . 127 6.3 Analysis . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 129 6.3.1 Reconstruction Quality . . . . . . . . . . . . . . . . . . . . . . 129 6.3.2 Effects of Loss and Mismatched Port Coupling . . . . . . . . . 131 6.3.2.1 Effect of Loss on Reconstruction . . . . . . . . . . . 131 6.3.2.2 Mismatched Port Coupling . . . . . . . . . . . . . . 134 6.3.3 Synthetic Sona Duration Constraint . . . . . . . . . . . . . . . 136 6.4 Conclusion . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 141 7 Exciting Reflectionless Unidirectional Edge Modes in a Reciprocal Photonic Topological Insulator Medium 142 7.1 Introduction . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 143 7.2 Design and Simulations . . . . . . . . . . . . . . . . . . . . . . . . . . 145 7.3 Experiment . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 146 7.4 Analysis . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 152 7.5 Ferrite Induced Non-reciprocity . . . . . . . . . . . . . . . . . . . . . 158 7.6 Conclusions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 159 8 Conclusions 160 8.1 Prior Works . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 162 8.2 Future Work . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 163 Appendices 165 Appendix A MATLAB Script For Generating Normalized Impedance Ensem- bles For 2-port Systems 166 Bibliography 171 v List of Tables 7.1 Summary of extreme transmisison values as deduced from experimen- tal data where TL and TR are transmission amplitude to left and right, respectively. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 158 vi List of Figures 1.1 Diagram of an electric power system; transmission system is in blue. [1] 2 1.2 Random Matrix Theory predictions for the Probability Density Func- tions of (a) Re[z] and (b) Im[z] as a function of increasing α, for a one-port time-reversal symmetric wave-chaotic cavity. Figure 2.3 in Ref. [2]. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 14 2.1 RCM-predicted probability density function of power ratios RN(α = 6) ≡ P (N) in /P (1) in for chains of up to seven cavities: the high-loss regime is assumed for all the (statistically identical) cavities in the chain. This is Figure 7 in Ref. [3]. . . . . . . . . . . . . . . . . . . . . . . . . 19 2.2 Electrical resistivity of copper vs. temperature. The different curves on the plot are the experimental results for different aluminum sam- ples and were measured with different techniques at different times from 1908 to 1981. (which is Figure 1 in [4]) . . . . . . . . . . . . . . 24 2.3 The schematics for the scaled cavity experiment setup. . . . . . . . . 28 2.4 Block diagram for Virginia Diode Inc frequency extender modules. (∗) Variable attenuator. (†) Isolator. Picture taken from VDI product manual [5]. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 29 2.5 A typical setup with VNA and VDI extenders for measurement. Pic- ture taken from VDI product manual [5]. . . . . . . . . . . . . . . . 30 2.6 The drawings (left), the outside vacuum can (middle) and the cooling plates inside of the cryostat (right). The cooling plates are cooled in a staged manner from 50K at the top to 10mK at the bottom. The sample will be mounted onto the 10 mK plate, also called the sample plate. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 32 2.7 The setup for high frequency waves to propagate in free-space from the frequency extender to the cavity, and from the cavity to the re- ceiving frequency extender. The horn antennas can efficiently launch and receive electromagnetic waves and the Teflon lens collimates the waves into a parallel beam. . . . . . . . . . . . . . . . . . . . . . . . . 34 vii 2.8 Magnetically coupled mode stirrer powered by a cryogenic stepper motor. The magnetic strip outside the cavity (lower yellow bar in the left side) is coupled by static magnetic field with the magnetic strip inside the cavity (upper yellow bar in the left side), eliminating the need for any hole on the wall. The upper right inset is an example of the mode stirrer placed inside the cavity. . . . . . . . . . . . . . . . . 39 2.9 The transmission amplitude in dB for free-space propagation mea- surement. The x-axis and y-axis are the distance between the lens to the transmitter antenna (d1) and the receiver antenna (d2) respec- tively. The yellow dotted circles enclose the region for best d1, d2 values for optimal transmission. . . . . . . . . . . . . . . . . . . . . . 43 2.10 Experimentally measured reflection (top two plots) and transmission (bottom two plots) magnitude for the s = 20 cavity for 5 realizations created by rotating the magnetically coupled mode stirrer. The left column plots the data in the full frequency range from 75 GHz to 110 GHz while the right column zooms in a 100 MHz window. Each curve is wildly different from others but yet follow the same slowly varying trend which is the non-statistical system specific feature. . . . 44 2.11 Power ratio Λ as a function of frequency and its histogram for a good ensemble (left) and a bad ensemble (right) data. Λ should have a large mean and a large dynamic range if the cavity modes are well perturbed and uncorrelated, which gives us a good ensemble of data. 45 2.12 Loss parameter α values for the full scale cavity measured by collabo- rators at U.S. Naval Research Laboratory. Each α value is calculated from experimental data in a 0.1 GHz window at the specified fre- quency. The data points are taken from Table 1 in [6]. . . . . . . . . 46 2.13 Probability Density Function (PDF) of the normalized impedance for a direct injection experiment on a scaled-down s = 20 copper cavity (dotted line), in comparison with the RCM Monte Carlo simulation with α = 4.5 (solid line). . . . . . . . . . . . . . . . . . . . . . . . . . 47 2.14 3D-printed model of the multiple connected cavities and the configu- ration for a 3-cavity cascade drawn in CST. . . . . . . . . . . . . . . 49 2.15 The air region of the 3-cavity cascade model with cavity walls and backplane omitted. The wave goes into the first cavity through the antenna mounting point, then couples into the second cavity mounted on the other side of the backplane (not shown) through an aperture. It is then coupled to the third cavity through the other aperture, and gets out through the antenna mounting point on the third cavity. . . 50 viii 2.16 A simple cascade of three scaled cavities. Top: the graph of the cascade, consisting of three nodes (scaled cavities) and two edges (apertures connecting two neighbor cavities). Bottom: the configu- ration of scaled cavities mounted onto the two opposing sides of a central plate. Green rectangles represent scaled cavities on the front side and blue rectangles represent scaled cavities on the back side. Orange circles represent apertures connecting the two cavities on the opposing sides. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 52 2.17 A network of seven scaled cavities. Top: the graph of the network, consisting of seven nodes (scaled cavities) and eight edges (aper- tures connecting two neighbor cavities). Bottom: the configuration of scaled cavities mounted onto the two opposing sides of a central plate. Green rectangles represent scaled cavities on the front side and blue rectangles represent scaled cavities on the back side. Orange cir- cles represent apertures connecting the two cavities on the opposing sides. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 53 3.1 The circuit model for a lossless (left) and a lossy (right) antenna. Zant is the input impedance of the antenna which is approximated by Zavg (which also includes short orbit effect in addition to Zant) in RCM normalization process, Zrad is the radiation impedance which describes the feature of the port, and R is the real part of Zrad that represent the power loss due to radiation. Figure 4, 5 in [7]. . . . . . 58 3.2 The inverse Fourier transform of the measured S-parameters give the value of τ from each fit in log-scale versus time. a) For the case of transmission and b) for the case of reflection of the s = 20 scaled en- closure measured through remote injection. Data from 9 realizations at room temperature are plotted with different colors. The purple line is the average, and the green line is the linear fit for the energy decay portion of the average. The slope of the fitted line is −1/2τ , where τ is the energy decay time of the cavity. The time domain re- sponse inside the blue dashed box in (b), labeled ’Prompt response’, arises from the impedance mismatch between the external transmis- sion channel and the cavity. This information is captured in Zavg. . . 67 3.3 Comparison between the normalized impedance PDF for a 2-port system from a RCM Monte Carlo simulation with α = 5.6, in solid lines, and that from a normalization process of experimental data with η11 = 0.14 and η22 = 0.19, in dotted lines. . . . . . . . . . . . . . 69 3.4 The comparison between the normalized impedance PDF from a di- rect injection experiment with an empty cavity (solid lines), and that from a one-sided remote injection experiment with an empty cavity (dotted lines). The remote injection data is processed using the radia- tion efficiency η11,absorber obtained from the one-sided remote injection with an absorber. . . . . . . . . . . . . . . . . . . . . . . . . . . . . 71 ix 3.5 A comparison between α values calculated from different methods as a function of time during a cycling of the dilution refrigerator hosting the scaled cavity. Blue solid line: calculated from time domain energy decay time method; Dotted lines: calculated from RCM normaliza- tion process with various values of η. . . . . . . . . . . . . . . . . . . 73 4.1 The full-scale cavity α measured by Zachary Drikas and Jesus Gil Gil at NRL with various number of absorbers inside. The left side plot is the average α for the whole frequency range, i.e. number of frequency segments N = 1. The right side plot is the α for N = 10 frequency segments. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 77 4.2 The fitting error for calculating the αN=10(f) values for the full-scale cavity is mostly around 0.05. The few high error data points are for α > αmax over the limit of the simulation α range. The right plot shows a typical case of the comparison between the PDF curves for the 5th frequency segment where the fitting error is 0.036164. . . . . . 78 4.3 The tunable range of α values by using different wall material and varying temperature. The least lossy wall material is polished copper, which gives a range of 2.6 ≤ α ≤ 4.2, including the αfull for full-scale cavity with 1/4 absorber in its range. The plotted α is calculated from the time-domain energy decay time τ . . . . . . . . . . . . . . . . 80 4.4 The horn antenna has higher gain at higher frequency band which results in higher radiation efficiency. Left plot taken from Virginia Diode, Inc documentation Nominal Horn Specifications [8]. . . . . . . 81 4.5 The frequency dependent loss parameter for the miniature cavity cal- culated from the time-domain energy decay time method, αQ, and from fitting with RCM simulation results, αfit. . . . . . . . . . . . . . 82 4.6 The comparison of PDFs for the normalized impedance Im[ξ21] for the full-scale cavity with 1/4 absorber, the miniature cavity at 103 Kelvin and the RCM simulation with α = 3.0. The experimental data is selected from the whole frequency range (N = 1), i.e. 3.75 ∼ 5.5 GHz for the full-scale cavity and 75 ∼ 110 GHz for the miniature cavity. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 84 4.7 Comparison of the probability density function (PDF) for the imagi- nary part of the normalized impedance ξ12 and ξ21 between the full- scale cavity (solid line based on data) and the miniature cavity (dot- ted line based on data) for three different frequency bands (of the full-scale cavity) at different temperatures (of the scaled cavity). Top row shows the PDFs in linear scale while the bottom row shows the same PDFs in log scale. (a) α = 2.83 within [4.45, 4.625] GHz at 130 Kelvin, (b) α = 4.19 within [4.975, 5.15] GHz at 217 Kelvin and (c) α = 5.82 within [5.325, 5.5] GHz at 297 Kelvin. Notice that in each plot, all four curves collapse into one because they match each other very well. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 85 x 4.8 The comparison of all 8 PDFs for the normalized impedances, the real and imaginary part of ξ11, ξ12, ξ21 and ξ22, for the full-scale cavity with 1/4 absorber and the miniature cavity. The experimental data are selected from [5.325, 5.5] GHz, the 10th segment of the N = 10 frequency segments, for the full-scale cavity and is selected from 297 Kelvin and [106.5, 110] GHz for the miniature cavity. . . . . . . . . . 87 4.9 The comparison of all 8 PDFs for the normalized impedances, the real and imaginary part of ξ11, ξ12, ξ21 and ξ22, for the full-scale cavity with 1/4 absorber and the miniature cavity. The experimental data are selected from [4.275, 4.45] GHz, the 4th segment of the N = 10 frequency segments, for the full-scale cavity and is selected from 90.1 Kelvin and [85.5, 89] GHz for the miniature cavity. . . . . . . . . . . 88 4.10 The distribution functions of the real (solid line) and the imaginary (dotted line) part of the normalized impedance ξ12 calculated from the RCM simulation for various α. The real and the imaginary part distribution functions are identical when α = 8 but start to differ when α = 5 and lower. . . . . . . . . . . . . . . . . . . . . . . . . . . 90 5.1 The complete computer 3D model for the multiple interconnected scaled cavity experiment setup. The details of each component visible here are discussed below. . . . . . . . . . . . . . . . . . . . . . . . . . 94 5.2 Scaled interconnected cavity design with aperture, antenna mounting hole and mounting screws. . . . . . . . . . . . . . . . . . . . . . . . . 96 5.3 Cross section of copper box wall showing the antenna mounting ar- rangement. The antenna is mounted to the box with an adapter plate. Concealed PEM studs are used to avoid having protruding screws or nuts in the box interior. . . . . . . . . . . . . . . . . . . . . . . . . . 97 5.4 One scaled cavity with two antenna installed is mounted on the cen- tral plate. Notice that the aperture is covered up since this is a single cavity configuration. . . . . . . . . . . . . . . . . . . . . . . . . . . . 98 5.5 The 3D models of one unit box with different insert configurations. Insert plates, shown in the upper right, can have two apertures (al- lowing the box to be coupled with two other boxes), one aperture (allowing the box to be coupled with another box as the end of a cascading chain of boxes) or no aperture at all (for a single cavity configuration). . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 99 5.6 3D model for a 3-cavity cascade setup. 3 unit boxes are mounted to opposite side of the center plate, connected through the apertures to form a cascade. Electromagnetic waves come in from a receiving antenna, passes through all 3 boxes in the cascade and go out through the other antenna. . . . . . . . . . . . . . . . . . . . . . . . . . . . . 101 5.7 Center plate model with apertures and clear screw holes. The notch at the top of the plate is to accommodate the antenna and lens. . . . 102 5.8 Perturber assembly 3D model. . . . . . . . . . . . . . . . . . . . . . . 104 5.9 Perturber assembly. . . . . . . . . . . . . . . . . . . . . . . . . . . . . 105 xi 5.10 Another view of a 3-cavity cascade setup. The 1X3 opening, the lens and antenna are aligned with the cryostat window to ensure maximum transmission of mm-waves. The grid of small green slots are for rotating gears (shown as red gears in upper right figure) to rotate magnetically coupled perturbers inside the cavity. A special plate can be installed within the 1X3 opening to mount gear if needed.106 5.11 Antenna adapter model. An adapter plate (rectangular blue plate) is required to mount the antenna (blue cone) and the lens holder (green) onto the cavity (red box). The antenna and lens can be installed onto the adapter plate first, as shown in the upper left figure. Then the adapter plate is mounted onto the cavity by PEM studs (small red cylinder in upper left figure), which do not require screw holes or any protrusion into the cavity. . . . . . . . . . . . . . . . . . . . . . . . . 108 5.12 Stepper motor mounting location. . . . . . . . . . . . . . . . . . . . . 109 5.13 Smooth mirror-like finish from sheet copper. The part comes with a protective plastic film that can be peeled away to reveal the metal surface that is free of milling marks. . . . . . . . . . . . . . . . . . . . 114 5.14 A side by side comparison for a 3-cavity cascade setup with the scaled- down cavities on left and full scale cavities on the right. Figure 6 in [9]116 5.15 Comparison of the PDF of the induced voltage on a 50 Ohm load attached to the last cavity between the scaled cavity cascade and its full-scale counterpart. Figure 4 in [9]. . . . . . . . . . . . . . . . . . . 118 6.1 Calculation of a brief synthetic sona from four simple orbits in a representitive 2D 1/4-bow-tie billiard. We first calculate a scaled and time-delayed version of the input signal, which is a Gaussian pulse modulation of a 7 GHz carrier signal in this example. These waveforms are summed to obtain the synthetic sona shown at the bottom. The two ports are 17.5 cm apart. . . . . . . . . . . . . . . . 125 6.2 (a) Physically measured sona, and (c) synthetic sona signal calculated from orbits less than 4 m (= 10 √ A) in length, and their time reversal reconstruction signals, (b) and (d), respectively. Only the upper half of the signals are plotted since they are essentially symmetric about the time-axis. The upper inset shows closeups of the initial Gaussian pulse (left, blue), the measured sona reconstruction (middle, green) and the synthetic sona reconstruction (right, red). The bottom inset plots some of the orbits used to calculate the synthetic sona. The horizontal and vertical straight walls of the billiard have lengths of 43.18 cm and 21.59 cm, and the two ports are 17.5 cm apart. . . . . 128 xii 6.3 Measured signals in cut-circle cavity in the measured sona time- reversal process. The sona signal in the cavity normal (green, shorter in time) and superconducting (blue, longer in time) states, and time- reversal reconstruction in the cavity normal (cyan, lower amplitude) and superconducting (red, higher amplitude) states. The sonas are generated by injection of a Gaussian pulse with 6σt = 3ns, modulat- ing a 7 GHz carrier signal. Data is taken at 6.4 K (superconducting state) and room temparature (normal state). . . . . . . . . . . . . . . 133 6.4 Reconstruction quality (Vpp and focus ratio) and |S21|2 statistics (µ and σn) measured in the 1/4-bowtie billiard as a function of carrier frequency: (a) (b) when no noise is added; (c) (d) when 2mV Gaussian random noise is added to the sonas and reconstructions. (a) (c) use the physically measured sona method, while (b) (d) use the synthetic sona method. All quantities are plotted normalized to their maximum values. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 137 6.5 Normalized reconstruction quality (normalized to its saturation value) for the physically measured and synthetic sona methods when a win- dowing function is applied to the sona before being time reversed, so that only the beginning part of the sona is used for the time backward step. The peak-to-peak voltage of the reconstruction is shown in (a) while the focus ratio is shown in (b). “MEA” and “SYN” refer to the physically measured and synthetic sona methods, respectively. “in- sert1” and “insert2” are two variations of the bowtie cavity geometry when inserts are added, as shown in the inset. . . . . . . . . . . . . . 140 7.1 Figure 1 in Ref. [10]. BMW as a photonic topological insulator. (a) Schematic of the BMW. Part of the top metal plate is removed to reveal the bed-of-nails structure below. The enlarged regions on the right illustrate the origin of the bianisotropic response. Right inset: an equivalent way to produce bianisotropy by adding an asymmet- rically placed metallic volume (washer) around the rod. (b) PBS of spin-degenerate metawaveguide with TE and TM modes forming doubly degenerate Dirac cones at K points. (c) Field profiles of the degenerate TE and TM mode at the K point. Colors: energy density. Arrows: electric field for the TM mode and magnetic field for the TE mode. Yellow dashed line: metallic border. (d) PBS with the band gap induced by the bianisotropy of the metawaveguide. Dashed lines in (b) and (d): TE and TM bands of interest. . . . . . . . . . . . . . 148 7.2 (a): Numerically calculated band structure of the waveguide, where four edge modes have been labeled. (b) to (e): Field profile |Hx−iHy| of the four edge modes at 6.13GHz (shown in (a) as a dashed line). It is clear that only the two spin-up states (from the two valleys), but none of the spin-down states, can be excited by a right circularly polarized magnetic dipole. . . . . . . . . . . . . . . . . . . . . . . . . 149 xiii 7.3 (a) Schematic of the experimental setup. ∆em is the bianisotropy coefficient [10] and the interface is defined by the boundary of the two regions with ∆em of opposite sign, denoted by a red dashed line. (b) Photograph of the top of the BMW structure showing the cor- responding elements in (a). The inset shows the arrangement of the two loop coils which are in the air gap of a cylinder at the interface. . 150 7.4 Transmission amplitude at the (a) left and (b) right side of the BMW interface as a function of frequency while varying the phase difference φ of the two driving loop antennas. The probe is positioned at the center of the edge. The BMW bulk band gap extends from 5.80 GHz to 6.47 GHz, as shown with the vertical dashed lines. . . . . . . . . . 152 7.5 Simulated BMW structure with TPSW-supporting interface in CST with 16 period long and 8 period wide graphene-like lattice structure of rods. The two loops making up the rotating magnetic dipole an- tenna are perpendicularly placed with two independent driving coax- ial cable inputs. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 154 7.6 CST simulation results for transmission amplitude to the left and right side of the BMW structure while varying both the phase differ- ence φ and driving amplitude (parameterized by angle θ ∈ [0, π/2]) of the two loop antennas. Results are shown for (a) left, (b) right 6.47 GHz and (c) left, (d) right 6.08 GHz. . . . . . . . . . . . . . . . 155 7.7 Transmission amplitude to the (a) left and (b) right side when varying both the phase difference φ and the input power (parameterized by θ) of the two loop antennas as deduced from the data at a frequency of 6.38 GHz. To examine the directivity, we plot the ratio of (c) left to right side and (d) right to left side transmission amplitude (in dB) as a function of θ and φ. . . . . . . . . . . . . . . . . . . . . . . . . . 157 xiv List of Abbreviations α Alpha. The dimensionless loss parameter in Random Coupling Model ξ The normalized impedance. Sometimes also denoted as z z The normalized impedance. Sometimes also denoted as ξ Zcav Measured cavity impedance Zavg Ensemble average of Zcav Zrad Radiation impedance of the antennas, or ports Zant Input impedance of the antennas, or ports Zant includes both Zrad and the antenna’s internal loss and delays BMW Bi-anisotropic Meta-Waveguide BTRS Broken Time Reversal Symmetry CNAM Center for Nanophysics and Advanced Materials CST Computer Simulation Technology, a numerical simulation software FDTD Finite-Difference Time-Domain IACS International Annealed Copper Standard IREAP Institute for Research in Electronics and Applied Physics LCP Left Circularly Polarized NRL Naval Research Laboratory OFHC Oxygen-Free High Conductivity ONR Office of Naval Research QHE Quantum Hall Effect QSH Quantum Spin Hall RCM Random Coupling Model RCP Right Circularly Polarized RMT Random Matrix Theory TE Transverse Electric TM Transverse Magnetic TPSW Topologically Protected Surface Wave TRS Time Reversal Symmetry VDI Virginia Diodes Inc VNA Vector Network Analyzer xv Chapter 1: Introduction and Overview 1 Figure 1.1: Diagram of an electric power system; transmission system is in blue. [1] 1.1 Background Wave propagation in various complex media is an interesting and practical field that has a huge impact in our daily life. One basic type of wave propagation is guided waves through carefully engineered and manufactured media, such as waveg- uides and transmission lines. For example, high frequency electromagnetic waves carrying encoded information in optical fibers can travel vast distances in seconds, providing the backbone of internet that connects the world. As another example, electric power transmission relies on a mesh of transmission lines to transfer electric power generated from power plants to users across the globe, providing the crucial infrastructure of modern society. Over the decades, research and engineering efforts has been made to optimize wave propagation properties in such media to better suit our needs. The most com- monly seen highly-engineered wave propagation medium in our daily life is probably the optical fiber, a widely used waveguide to transmit light over long distances for high bandwidth communication. In this case, we want to have lower insertion loss 2 such that the signal quality can be maintained with less re-amplification [11–13], thus traversing longer distances without loss of signal fidelity. People also explored single-mode fiber vs. multi-mode fiber for different use cases considering the travel distance and bandwidth, invented new materials to achieve better properties com- pared with the conventional silicon dioxide, or even to acquire entirely new novel properties [14–17]. Another common type of wave propagation is in a confined medium, such as inside a room, a building or in general any partially open enclosure. Its applications includes telecommunication, sensors and wireless power transfer. One major differ- ence with guided waves is that we typically do not try to control the details of the enclosure, which makes sense since we would like our WIFI to work regardless of which room I am standing in and what objects are placed around. Instead, we are interested in the generic statistical properties of the wave transmission in enclosures categorized by generic properties, such as the volume or the material making up the walls, as opposed to the exact shape or other specific conditions. 1.2 Thesis Overview In this thesis, I study both of the above two types of wave propagation with exper- imentation and compare them with simulation and theoretical results. For wave propagation within enclosures, we measured the transmission prop- erties of electromagnetic waves inside metal cavities, launching and receiving mi- crowave signals through antennas mounted on the cavity walls. To imitate the 3 propagation of microwave signals used in telecommunication frequency ranges (typ- ically 1 ∼ 6 GHz) inside a typical building, we scaled down an otherwise enormous metal structure spanning several rooms into small metal boxes that could be man- aged, configured and integrated into our experimental setup. In this thesis, I discuss the practical challenges of scaling down the cavities in Chapter 2, explore the prop- erties of the antenna on the transmission measurements in Chapter 3, verify my experimental methodology with a single cavity setup in Chapter 4, then applied it on a more complex multiple connected cavities setup in Chapter 5. Although it is mentioned above that our focus is on the cavity’s statistical properties, which are independent of the exact geometric details, it is nevertheless interesting to explore what we could achieve if the geometric information of the cavity boundaries is known. Specifically, we’d like to see if we could construct a signal based on the geometry information alone and broadcast it from one antenna to another such that it would focus in space and time at the second antenna. At first glance, the geometric information seems simple to obtain. After all, we man- ufactured all the cavities according to our own design specifications. However, the actual geometry could vary with lots of uncontrollable factors, e.g. room tempera- ture changing the volume of the cavities, warping of the cavity walls, differences in surface condition due to dust, oil, or other residues, etc. So the effectiveness of our constructed signal decreases as it bounces off the cavity walls more and more as it travels. We discuss our findings in Chapter 6. Finally, as a case study for guided wave propagation, we looked into the emerg- ing new type of materials, photonic topological insulators, which are an interesting 4 class of materials whose photonic band structure can have a band-gap in the bulk while supporting topologically protected unidirectional edge modes. In Chapter 7, we performed experiments on a 2D waveguide composed of hexagonal graphene-like lattice. The resulting electromagnetic waves traveled from the source antenna, along the waveguide, to the two sides in a reflectionless manner, i.e. there’s no reflection or back scattering of waves. But before we delve into the topics in this thesis, there are some fundamental theories and prior work that need to be discussed first. 1.3 Ray-chaotic Cavities The property of waves coupling into and propagating inside an electrically large complex enclosure is of interest to several fields. In electromagnetic compatibility (EMC) the goal is to minimize the coupling by providing better shielding and thus lower the chance of a larger induced voltage on sensitive devices located inside the enclosure, thus minimizing potential damage. In telecommunications one would like to maximize the coupling and the induced voltage to boost up the transmitted signal inside an enclosure, which could be a room with windows and doors. These enclo- sures are modeled as ray-chaotic cavities, where waves are very sensitive to geometry details and small changes, which is the case for most real life situations. Thus a statistical description is more approachable and applicable than trying to calculate an exact solution of the problem. In light of this, the Random Coupling Model (RCM) was introduced by Zhang et al., as a method to predict the statistical dis- 5 tribution of the induced voltages at locations inside a ray-chaotic enclosure [18,19]. It combines the universal predictions from Random Matrix Theory (RMT), briefly introduced below in section 1.4, and the system-specific properties characterized by the system’s port radiation impedances. Complex enclosures, such as computer cases with circuitry inside, or offices filled with desks, chairs, and electronics, are examples of ray-chaotic systems. To define what we mean by ray-chaotic, consider the case where the wavelength is short and a ray description is appropriate. Consider two rays starting from the same location in such an enclosure but with slightly different directions. As the rays propagate, reflecting from either curved surfaces or the interior features of the enclo- sure, their separation will tend to increase exponentially in time, and we call such a situation ray-chaotic. Ray chaos leads to an extreme sensitivity to initial conditions for the rays [20]. For waves propagating in highly over-moded ray-chaotic struc- tures, the exact solution for the fields depends strongly on the geometric details of the structure and is very sensitive to small changes in frequency or geometry. Thus, in the presence of even small uncertainties in structure or frequency, a statistical approach may be more appropriate than trying to obtain an exact solution for field quantities inside the structure [21]. The Random Coupling Model (RCM) is one such method to predict the statistical properties of the waves inside a ray-chaotic enclosure [18, 19]. The RCM has been widely discussed and tested over the years, with good agreement between theory and experimental results on individual complex structures [2, 3, 6, 7, 22–24]. It has also been used to study the effect of a non-linear port on the measured statistical electromagnetic properties of a ray-chaotic complex 6 enclosure in the short wavelength limit [25]. 1.4 Random Matrix Theory The RCM is based on Random Matrix Theory, originally proposed to model the energy level statistics of heavy nuclei [26]. The idea is that if the wave system is sufficiently complex then its fluctuating properties have the same statistics as those of a suitable ensemble of random matrices [27] (hence the name ”Random Matrix Theory”). Certain statistical properties, such as the distribution of the normalized spacings between nearest neighbor eigenfrequencies (ε), follow a universal behavior regardless of the system details. The type of random matrix is chosen according to the general symmetry of the system in order to correctly represent its dynamics. For instance, the Gaussian Orthogonal Ensemble (GOE) describes systems with Time-Reversal Symmetry and the Gaussian Unitary Ensemble (GUE) describes systems with Broken Time-Reversal Symmetry. It is later conjectured [26,28–32], and validated in some cases [27,33–35], that most wave-chaotic systems follow random matrix statistics for a properly chosen ensemble, giving Random Matrix Theory a broad range of applications. 1.4.1 Random Matrices Random Matrices are matrices whose elements are random variables. If we take one realization for each of the random variables and group them together as a matrix, then we get one realization of the random matrix. Taking many such realizations is 7 called an ensemble. The two random matrices relevant to electromagnetic systems are Gaussian Orthogonal Ensemble (GOE) and Gaussian Unitary Ensemble (GUE) corresponding to systems with Time-Reversal Symmetry (TRS) and Broken Time- Reversal Symmetry (BTRS) respectively. • For a GOE matrix, each element, Xi,j, is a real independent-identically-distributed (i.i.d) Gaussian random variable with zero mean. All the off-diagonal ele- ments have a variance of 1/2 while the diagonal ones have a variance of 1, i.e. Xi,j ∼ N(0, 1 2 ) for i 6= j and Xi,i ∼ N(0, 1). • For a GUE matrix; It is a Hermitian matrix with real diagonal elements and complex off-diagonal elements. Each diagonal element is a real i.i.d Gaussian random variable with zero mean and unit variance, i.e. Xi,i ∼ N(0, 1). The off-diagonal elements are complex with real and imaginary parts both being i.i.d Gaussian random variable with zero mean and 1/2 variance, i.e Xi,j ∼ N(0, 1 2 ) + iN(0, 1 2 ) for i < j. Once an appropriate random matrix is constructed, its eigenvalues can be calculated and then used to study the statistical properties of the corresponding wave-chaotic system, such as the normalized spacings between the nearest eigenfrequencies. 1.4.2 Normalized Spacings Between The Nearest Eigenfrequencies In the case of electromagnetics, the normalized spacings between the nearest eigen- frequencies is defined as ε = (k2 n+1− k2 n)/(∆k2 n) where kn is the nth eigenfrequency’s wavenumber, and ∆k2 n = 〈k2 n+1 − k2 n〉 is the mean spacing between eigenlevels. For 8 a given enclosure whose size is much larger than the wavelength, the mean spacing can be calculated as ∆k2 n ∼= 4π/A (2D) ∼= 2π2/(kV ) (3D) (1.1) where A and V are the area and volume of the 2D or 3D cavity. Then according to the RMT, the probability density function (PDF) of ε for different enclosures follows one of the two universal curves, depending on whether the system has Time Reversal Symmetry (TRS) or Broken Time Reversal Symmetry (BTRS): P (ε) ∼= π 2 εe−πε 2/4 (TRS) ∼= 32 π2 ε2e−4ε2/π (BTRS) (1.2) These are called “Wigner distributions” and they are proven to be applicable to various wave-chaotic systems. Note that P (0) = 0 in both cases, meaning that all degeneracies are broken in pure RMT systems. 1.5 Random Coupling Model Random Matrix Theory (RMT) provides a universal statistical prediction for the generic properties of wave-chaotic systems, however it is difficult to identify these universal statistical properties in experimentally measured data because it inevitably contains system-specific features like the coupling between the ports and the cavity modes and short orbits [36–38]. The Random Coupling Model (RCM) introduces a framework to incorporate the non-universal features with the universal statistical 9 properties of appropriate random matrices to reproduce in the statistical sense the experimentally measured cavity impedance matrices. The effect of uniformly dis- tributed loss in the system is to create a sub-unitary scattering system [39], and this effect is captured to very good approximation by a single loss parameter α [18, 19]. The RCM is formulated in terms of the impedance matrix Z of an N -port system in analogy to the reaction matrix in nuclear scattering theory [40–45]. The ports represent sources or sinks of radiation that introduce or absorb energy in the enclo- sure. The impedance relates the voltage induced on one port to the currents at all of the N ports, and is simply related to the N × N scattering matrix S through a bilinear transformation S = Z 1/2 0 (Z + Z0)−1(Z − Z0)Z −1/2 0 , where Z0 is a diagonal real matrix whose elements are the characteristic impedance of the transmission line modes connected to each port. Similar to RMT, the loss parameter α defines the universal statistical property of the normalized impedance matrix, z (sometimes also denoted as ξ), which is a key parameter to describe any electromagnetic enclosure. α is defined as α = k2/(∆k2 nQ) where Q is the unloaded cavity quality factor. If we plug in Equation (1.1) for 2D and 3D systems, α can be written as α = k2A 4πQ (2D) = k3V 2π2Q (3D) (1.3) 10 1.5.1 S-parameters & Z-parameters For an electromagnetic system, waves are coupled into or out of the system through ports. An N port passive electromagnetic network is usually described by a N -by-N scattering matrix S (S-parameters) or impedance matrix Z (Z-parameters), which are both well-established quantities in microwave engineering. The S-parameter element Si,j is the complex ratio of the amplitude and phase of the outgoing wave at port i to the amplitude and phase of the incoming wave at port j when only the jth port has a nonzero incoming wave while all other ports are terminated with a matched reflectionless load, i.e. Si,j = bi aj |am=0,m 6=j, where ai, bi are complex numbers representing the incoming and outgoing wave at port i respectively. Similarly, the Z-parameter element Zi,j is the ratio of the induced voltage at port i to the source current at port j when only the jth port has nonzero source current, i.e. Zi,j = Vi Ij |Im=0,m 6=j, where Vi, Ii are the voltage and current at the ith port respectively. In a typical microwave experiment, one uses a vector network analyzer to measure the cavity S-parameters, which can be converted into the cavity Z-parameters by Z = Z 1/2 0 (I + S)(I− S)−1Z 1/2 0 , where I is an identity matrix, Z0 is a diagonal matrix whose elements, Zi,i, are the characteristic impedances of the transmission line connecting to the ith port (typically 50 or 75 Ohms for a coaxial cable). To couple waves into or out of an enclosure, an antenna is required which usually presents an impedance mismatch 11 with the connected transmission line. The mismatch causes the incoming waves to partially reflect back and also prevents the antenna from picking up waves inside the enclosure efficiently. This is an inevitable system-specific feature that exists in almost all microwave experiments, resulting in a deviation from the expected RMT universal behavior when analyzing the experimental data. 1.5.2 Normalized Impedance To remove the system-specific features, the Random Coupling Model uses a non- statistical impedance matrix, Zavg, which is obtained by averaging the measured cavity Z-parameters Zcav over many realizations, to characterize the system-specific properties and to normalize the experimental data. It is expected that the universal fluctuations cancel out in the ensemble average because 〈Re[Z]〉realization = 1 and 〈Im[Z]〉realization = 0. Realizations of the same cavity are created by perturbing the cavity modes while retaining the same cavity volume, usually by rotating a large irregularly-shaped metal panel. Zavg mainly includes the radiation impedances of the antennas which characterize the mismatch mentioned above, and it also includes the influence of non-statistical short orbits between the ports, as discussed in [38]. Once we obtain Zavg = 〈Zcav〉realizations, the RCM suggests normalizing the measured Zcav by ξ = (Re[Zavg])−1/2(Zcav − jIm[Zavg])(Re[Zavg])−1/2 (1.4) This quantity ξ, sometimes also simply called z in some papers, is expected to have the statistical properties predicted by RMT for some value of loss parameter α. 12 1.5.3 Loss Parameter α Similar to Random Matrix Theory, the statistics of the normalized impedance ξ follows a universal curve defined by the loss parameter α, which can be calculated according to Equation (1.3). Figure 1.2 (which is Figure 2.3 in [2]) illustrates the statistics of ξ for a one-port system with different α values. The statistics are not calculated by traditional electromagnetic simulations that solve Maxwell’s equations inside a particular enclosure. Instead, the statistics are obtained by Monte Carlo simulations by constructing many random matrices following RMT, and examining their statistics. In practice, it is usually difficult to obtain an accurate estimate for the unloaded quality factor of the cavity, thus alternative methods are employed to determine α. For example, in the high loss regime (α > 5), the variance of the normalized impedance can be expressed as σ2 Re[ξ] ≈ σ2 Im[ξ] ∼= 1 2πα (BTRS) ∼= 1 πα (TRS) (1.5) Hence, one can conduct experiments to measure Zcav for many realizations, nor- malize them to get ξ then use Equation (1.5) to calculate α. More generally, α can always be determined by finding the universal curve defined by α that best fit the statistics of ξ, which is obtained through experiment. The universal impedance statistics curves only depend on α values and can be calculated by methods pre- sented in [2] Chapter 2.5. 13 Figure 1.2: Random Matrix Theory predictions for the Probability Density Func- tions of (a) Re[z] and (b) Im[z] as a function of increasing α, for a one-port time- reversal symmetric wave-chaotic cavity. Figure 2.3 in Ref. [2]. A complete list of methods to estimate cavity α is presented in Ref. [2] Ap- pendix B. 1.5.4 Extensions of RCM The RCM provides a framework to analyze the statistical properties of wave-chaotic systems, taking into account the universal properties, the loss parameter α, and the system-specific properties. However, it only covers single-cavity linear systems. In real life scenarios, this means that RCM can be used to study the wave properties inside, say, a room, but it requires additional steps to study interconnected cavities, such as the floor of a building consisting of multiple rooms connected with doors and hall ways, with each room potentially having its own unique geometry and properties. In Chapter 5, we look into this case by extending RCM to model multiple connected cavities. There are also situations where nonlinear behavior is added to the mix, for 14 example when an amplifier or p/n junction-based electronics is present in the room. Nonlinearity adds complexity to the system, making the modeling of the system more difficult, but is nevertheless an interesting property that often opens avenues for novel applications not only in electromagnetic waves [46], but also in other areas such as elastics waves [47] and gravity waves [48]. Extending RCM into nonlinear systems, Min Zhou added an active nonlinear circuit which generates strong second harmonic waves into a quasi-2D wave-chaotic billiard in [49]. The study showed that the statistics of the harmonics can be predicted by modeling the nonlinear cavity as two cascaded linear cavities connected by a nonlinear circuit. 15 Chapter 2: Testing The Random Coupling Model Predictions in a Scaled-Down Cavity With Remote Injection Setup 16 There is interest in using the RCM to understand the wave properties of more complex structures, such as a cascade or a network of coupled cavities [50, 51]. It becomes increasingly difficult to experimentally test these structures due to their large size and the difficulty in managing and reconfiguring them in a typical labo- ratory environment. To solve this problem, we propose miniaturizing the complex structure while maintaining the statistical properties of the waves by carefully scal- ing the frequency and the quality factor of the system. Electromagnetic geometric scale modeling has been used extensively in simulations and modeling of large struc- tures for decades [52–54]. It is also routinely done in other fields such as ship model testing [55] and wind tunnel testing [56] where a miniature model is constructed and studied for design verification . The idea of scaling down the geometric size is not new in modeling, but the challenge is to make other electromagnetic properties scale appropriately as well. In Chapter 2, we discuss the practical challenges of testing the theory in ex- periment, explain how the scaled cavity setup works and introduce the experimental setup. In order to analyze the experimental data, we need to modify the RCM to accommodate the case with lossy ports, which is discussed in Chapter 3. Then in Chapter 4 we validate this setup by comparing the single miniature cavity result with the single full-scale cavity result obtained by our collaborators at the Naval Research Laboratory (NRL). Finally we expand the setup to have multiple cavities coupled through apertures, and present the experimental result in Chapter 5 17 2.1 The Need For Scaled Cavities Many RCM predictions have been successfully tested in experiments and it is still expanding to include more complex scenarios. In this project, we are interested in the RCM prediction for connected cavities, as discussed in [3,24]. A chain of coupled ray-chaotic cavities represents many common situations, such as the compartments in a ship and offices and hallways in a building. RCM predicts the statistics of the induced voltages for ports located in each cavity along the chain as a function of the loss and the coupling. Figure 2.1 shows the predicted ratio of the power coupled into the N th cavity over the power coupled into the first cavity, as a function of N for serially connected α = 6 cavities. However this theoretical result is hard to verify in experiment since it requires a huge space to host the connected cavities, and many decades of dynamic range of microwave power measurement. The previous experimental setup for a single over-moded cavity with volume V ≈ (20λ)3 is about 1m3 and it would be difficult to fit in even a few cavities in the limited university lab space. Hence we introduced a scaled cavity experiment setup that can host a chain of cavities with total volume V ≈ (450λ)3. The basic idea is to scale down the cavity size and, in order to keep Maxwell’s equations unchanged, scale up the frequency of the electromagnetic waves and conductivity of the cavity walls. We’ll discuss the details of the scaling in Section 2.2, its implementation in Section 2.3 and present a series of progressive experiments to help understand and test the operation of this setup. 18 Figure 2.1: RCM-predicted probability density function of power ratios RN(α = 6) ≡ P (N) in /P (1) in for chains of up to seven cavities: the high-loss regime is assumed for all the (statistically identical) cavities in the chain. This is Figure 7 in Ref. [3]. 19 2.2 Scaling of The Cavity The main purpose of the scaling is to shrink the cavities down in linear size by a factor of s, i.e. V ′ = V/s3, and create a scaled-down-in-size version with the same statistical electromagnetic properties. Note that each individual mode in the full scale enclosure will not be reproduced precisely in the miniature version. Instead, the statistical properties should be identical before and after the scaling. We are targeting scaling factors of s = 20 and s = 40. We would also like to make this a manageable, reconfigurable and extendable experimental setup. In this section, we will discuss the necessary scaling of the frequency and cavity wall conductivity in order to maintain the same α value, and thus the same statistical properties. 2.2.1 Frequency Scaling The need for frequency scaling is obvious: when the cavity is scaled down in size by a factor of s the wavelength must also scale down by s in order for the cavity to remain the same electrical size. If volume is scaled down to V ′ = V/s3 and V = (Nλ)3, we need V ′ = (Nλ′)3, where λ and λ′ are the wavelength before and after the scaling respectively. Thus wavelength is scaled down by s, λ′ = λ/s, and the frequency f = c/λ is scaled up by s. Frequency scaling can be achieved by using frequency extenders which are frequency multipliers that convert signals from 0 ∼ 10 GHz (microwave) to the several hundred GHz range (mm-wave). After scattering, the signals are received and then mixed down to 0 ∼ 10 GHz so that they can be measured by a microwave 20 Vector Network Analyzer (VNA). The proposed setup uses extenders that are in the range of 75 ∼ 110 GHz (WR10 band) and 220 ∼ 330 GHz (WR3.4 band), which correspond to the scaling of s = 20 from 3.75 ∼ 5.5 GHz and s = 40 from 5.5 ∼ 8.25 GHz. 2.2.2 Cavity Wall Conductivity Scaling As stated in Equation (1.3), since α ∝ k3V/Q must remain unchanged, and that k3V remains the same for the given cavity, the quality factor Q must be the same as the full-scale cavity. The quality factor is defined in general as the ratio of the energy stored to the energy dissipated per cycle on resonance. When the wavelength is much smaller than the system size, the quality factor of an empty metallic enclosure with loss dominated by ohmic loss in the walls can be estimated as Q ≈ 3 2 V Sδ , where S is the wall surface area, δ = √ 2/(ωµσ) is the skin depth in the local limit, and σ is the electrical conductivity. δ is the depth that the electromagnetic waves can penetrate into the metal before the induced current screens out the incident wave. Ohmic loss within the skin depth is the main cause of energy loss in our cavities. In the local limit, the skin depth is related to the conductivity σ by δ = √ 2/(ωµσ), where ω = 2πf is the angular frequency, µ is the magnetic permeability of the conductor. Putting this into the expression for Q and then putting Q into the expression for the RCM loss 21 parameter α ∝ k3V/Q, we have α ∝ k3S √ ωµσ . (2.1) If we only look at the scaling with respect to s, we can further apply k ∝ s, ω ∝ s, S ∝ 1/s2, which leads to α ∝ s3(1/s2)√ sσ = √ s/σ. (2.2) Therefore, the conductivity of the wall must also be scaled by a factor of s in order to keep the RCM loss parameter α the same after the scaling. This is required to have the same fluctuating statistical properties in the scaled and un-scaled cavities. In theory, the electrical resistance of a metal changes with temperature in two regimes [57]: • At room temperature the change in resistance is proportional to the change in temperature: ∆R = R0αR∆T , where ∆R is change in resistance, ∆T is change in temperature, R0 is resistance at the reference temperature and αR is the temperature coefficient of resistance (not to be confused with the loss parameter α in the Random Coupling Model). Typically a metal’s resistance goes up as temperature goes up, i.e. αR is positive, since collisions between vibrating atoms and conduction electrons happen more frequently. • At low temperature the resistance is dominated by impurities or defects in the material and becomes almost constant with temperature. In experiment, conductivity scaling can be achieved by a combination of meth- 22 ods: • Cool down the cavity to low temperatures using a cryostat, • Change the cavity wall material to a better conductor, such as from aluminum to Oxygen Free High Conductivity (OFHC) copper, • Reduce surface roughness by physical polishing of the cavity interior surfaces. First we put the metal cavity in a cryostat that can bring down the temperature to about 10 Kelvin. The electrical resistivity of aluminum ρAl vs. temperature is shown in Figure 2.2 (Figure 1 in [4]) with different samples and measurement techniques. It is clear that ρAl is decreasing as temperature goes down but the curve eventually saturates at some value ρsat Al . The saturation value are different for different curves, which are the result of measuring different samples. In general, the higher the purity, the lower the ρsat Al value. So ideally by choosing a suitable aluminum material, we can achieve more than s = 40 scaling by cooling down to a certain low temperature, before reaching the superconducting transition of aluminum (which happens around 1.2 Kelvin). During the cavity design, we discovered that commercially available aluminum may not have a high enough conductivity scaling range to match the s = 40 scaling, i.e. their ρsat Al value is not low enough. This is mainly due to the added impurities in the aluminum alloy that lead to higher ρsat Al but are required to maintain certain de- sirable mechanical properties. So instead of using aluminum as the cavity material, we chose OFHC copper which has a lower ρsat Cu value. 23 Figure 2.2: Electrical resistivity of copper vs. temperature. The different curves on the plot are the experimental results for different aluminum samples and were measured with different techniques at different times from 1908 to 1981. (which is Figure 1 in [4]) 24 After changing to OFHC copper, it was found in experiment that the α value at the lowest temperature is still higher than what we expected, prompting more research into the factors that affect surface conductivity of metals. One simple method to increase the surface conductivity is to reduced surface roughness [58,59] by physically polishing the inside walls of the cavity. The 5-sided rectangular cavity, or the cup, is milled out from a piece of bulk metal, leaving a milling pattern on the inside walls. Although the surface feels smooth the milling pattern indicates that there are micro-structures that increases surface roughness. If the surface roughness is at the scale of the skin depth, the microwave surface losses will be enhanced [58,59]. After polishing it to a mirror finish, we observe a further decrease in the α value. An important constraint is that the polishing work is not at its best performance because it is difficult to put proper tools inside the solid 5-sided box. Thus in the future design of scaled cavities, it is best to start with a well-polished sheet metal and then fold it into a 5-sided cavity, which is the basis for my design for the multiple coupled cavities. The copper used in the 5-sided cavity is C10100 Oxygen- Free Electronic (OFE) copper, 99.99% pure copper with 0.0005% oxygen content and a minimum 101% IACS (International Annealed Copper Standard) conductivity rating. The copper used in the multiple-cavity design is C11000 Electrolytic-Tough- Pitch (ETP), the most common copper with 0.02% to 0.04% oxygen content and usually meets or exceeds the 101% IACS specification, and is mechanically polished to mirror-like finish. With these three methods combined, we are able to reduced the α value from about 6.5, at room temperature for the miniature aluminum cavity, to about 2.8, at 25 the lowest temperature for the polished copper cavity. The comparison is shown in Figure 4.3 2.2.3 Scaling Limits How far can we scale the cavities down in size? The current limiting factor for s to go beyond 40 is mostly the difficulty in further frequency scaling. As we will discuss in the following sections about the experimental setup, the corresponding frequency band for s = 40 is 220 ∼ 330 GHz, which is a very high frequency range for millimeter wave products such as frequency extenders, waveguides and horn antennas. Perhaps as millimeter-wave technology advances and matures, we could reach a scaling factor of 60, 80 or beyond. Another issue with scaling with larger values of s is the need to increase the wall conductivity by even greater amounts in the scaled structure. This is certainly possible if we start with full-scale systems having large values of RCM loss parameter α, for example 10 and larger. 2.3 Experimental Setup In our setup, we scale down a 66 cm by 122.5 cm by 127.5 cm aluminum “full-scale” cavity designed for the 3.7 ∼ 5.5 GHz range (WR187 band) by a factor of 20 in each dimension, i.e. s = 20. The scaled cavity is a rectangular box (6.375 cm X 6.125 cm X 3.300 cm with rounded corners) containing a perturber of irregular shape that can be rotated by motor control. The new (scaled) frequency range becomes 26 75 ∼ 110 GHz (WR10 band), which can be measured by using a Keysight network analyzer (KT-N5242A 10 MHz to 26.5 GHz PNA-X ) working together with two VDI frequency extenders (Tx/Rx WR10 module). To achieve higher Q, the miniature cavity is made of oxygen-free high-conductivity (OFHC) copper, with mechanically polished inner wall surface to reduce the surface resistance [58, 59]. We then use a custom-built BlueFors BF-XLD400 cryogen-free dilution refrigerator system, which can reach a base temperature of 10 mK under minimum heat-load conditions, to cool the cavity and further increase Q. The available volume for samples is a cylinder of 50 cm in diameter and 50 cm in height, that has a total volume of V ≈ (150λ)3 at 100 GHz, providing abundant space for larger structures. The following sections describe the detail of the above experimental setup in four parts: • Measurement system including a VNA and frequency extenders (2.3.1) to ex- tend the frequency range of VNA from 26.5 GHz to 330 GHz. • Cryostat to keep the sample in low temperature in order to achieve conduc- tivity scaling (2.3.2). • Free-space propagation path to inject the source signal (75 ∼ 110 GHz or 220 ∼ 330 GHz frequency range) into the sample cavity without direct waveg- uide connection (2.3.3), also called remote injection. • Magnetically coupled mode stirrer powered by a cryogenic stepper motor to generate multiple realizations of the cavity by perturbing the cavity modes (2.3.4). 27 Figure 2.3: The schematics for the scaled cavity experiment setup. The schematics of the setup is shown in Figure 2.3. 2.3.1 VNA & Extenders As mentioned in Section 2.2.1, we need frequency extenders to up convert the VNA source signal from around 10 GHz to hundreds of GHz, and then down convert the transmitted signal for the VNA to measure. The VNA that we are using is a 4-port Keysight N5242A PNA-X, a high performance model that works up to 26.5 GHz. The frequency extenders are made by Virginia Diode Inc, models WR10TxRx and WR3.4TxRx, whose block diagram is shown in Figure 2.4 (Figure 1 in [5]). The 28 Figure 2.4: Block diagram for Virginia Diode Inc frequency extender modules. (∗) Variable attenuator. (†) Isolator. Picture taken from VDI product manual [5]. “RF (L)” and “RF (H)” are input microwave signals generated by the VNA with relatively lower (L) or higher (H) frequency. The RF signal is first multiplied in frequency by a factor of N2 (for “RF (H)” input) or N1N2 (for “RF (L)” input) and then attenuated and sent through an isolatior to become the mm-wave input signal. A portion of the mm-wave signal is sampled out before sending to the test port, in order to be mixed down by the local oscillator (LO) signal, which is also multiplied in frequency by a factor of M . The resulting intermediate frequency (IF) fIF,Ref. = N1N2fRF(L) ±MfLO is in the range of 10 GHz, measurable by the VNA, and is measured at the “Ref.” port. The reflected mm-wave signal from the test port is sampled and mixed down in a similar fashion and is measured at the “Meas.” port. As discussed in Section 1.5 the S-parameters are complex ratios of amplitudes of the outgoing waves, measured at the “Meas.” port, to the incident waves, measured at the “Ref.” port. 29 Figure 2.5: A typical setup with VNA and VDI extenders for measurement. Picture taken from VDI product manual [5]. A typical setup with VNA and VDI extenders for measurement is shown in Figure 2.5 (Figure 10 in [5]). These models are chosen because they provide the best dynamic range in the global market, and since the loss during the transmission from one extender to the other is expected to be fairly high, especially when multiple cavities are connected, we must ensure that the dynamic range is large enough for the transmitted signal to stay above the noise level. 2.3.2 Cryostat A cryostat is an apparatus for maintaining a very low temperature. In our setup, we are using a custom made BlueFors BF-XLD400 cryogen-free dilution refrigerator system that can reach a base temperature of 10 mK under minimum heat-load 30 conditions. The space available for mounting samples is a cylinder of 50 cm in diameter and 50 cm in height, giving us a volume of V ≈ (450λ)3 at 300 GHz. For s = 40, we are scaling the frequency from 5.5 ∼ 8.25 GHz to 220 ∼ 330 GHz, and shrinking a geometry as large as V ≈ 253m3 into our cryostat. This is extremely difficult to achieve in full scale and also hard to operate and manage. Our scaled setup is an elegant solution to electromagnetic problems in such large scales. Figure 2.6 shows the drawings, the outside vacuum can and the cooling plates inside of the cryostat. The horizontal circular plates will be cooled down to 50K, 4K, 1K and 10mK from the top plate to the bottom plate, respectively. Our sample cavity will be mounted onto the bottom plate (the sample plate) which should reach the lowest temperature. There are several thermal shields designed to thermally isolate the cooling plate and a vacuum can at the outermost layer to provide a single vacuum space. Due to the need for a special free-space propagation path from extender to the sample cavity, there are windows on the side of the cryostat shields allowing electromagnetic waves to propagate in and out of the cryostat interior. These windows, allowing outside radiation to get inside, puts an extra heat load on the cryostat, which changes the lowest temperature that it can reach from 10 mK to about 10 K. However, this higher base temperature is still lower than we need for the scaled structure measurement. 31 Figure 2.6: The drawings (left), the outside vacuum can (middle) and the cooling plates inside of the cryostat (right). The cooling plates are cooled in a staged manner from 50K at the top to 10mK at the bottom. The sample will be mounted onto the 10 mK plate, also called the sample plate. 32 2.3.3 Free-space Propagation Path Since the miniature cavity is sitting inside the evacuated cryostat at low temper- ature, it is not possible to employ an input connection from the signal source to the cavity via a coaxial cable or waveguide. Accordingly, we use a quasi-optical free-space propagation path similar to that of a collimated beam in an optical ex- periment. The high frequency electromagnetic wave coming out of the frequency extender is launched into air by a horn antenna, then collimated by a Teflon lens. The output is a collimated beam propagating in free-space like a plane wave which has significantly lower loss compared to transmission in any waveguide or transmission line. The receiving end has a focusing lens, identical to the one on the source side, and a receiving horn antenna which is mounted on the wall of the cavity to transmit the received wave into the cavity. Two such free-space propagation paths are used for the two cavity ports, one path for each port. Figure 2.7 shows the experimental setup highlighting the free-space propagation path, the frequency extenders, the horn antennas, and the lenses. This free-space propagation path has its advantages and challenges compared to other methods. First of all, there is no direct thermal contact between the source and the cavity. This is the most crucial reason why we choose this setup. The cavity needs to be cooled to a low temperature inside the cryostat in order to achieve conductivity scaling. A direct connection, such as waveguide, will certainly prevent the cavity 33 Figure 2.7: The setup for high frequency waves to propagate in free-space from the frequency extender to the cavity, and from the cavity to the receiving frequency extender. The horn antennas can efficiently launch and receive electromagnetic waves and the Teflon lens collimates the waves into a parallel beam. 34 from cooling down by thermal conduction. Whereas this remote injection method only introduces some thermal radiation which can be lowered by proper filtering. Secondly, it is very low loss. Transmission lines and waveguides suffer from high loss at high frequency due to the scaling of ohmic loss and dielectric loss with frequency. The ohmic loss in metal is proportional to the surface resistance Rs = 1/(σδ) where σ is the conductivity and δ = √ 2/(ωµσ) ∝ 1/ √ ω is the skin depth. So Rs ∝ √ ω increases as frequency goes up, leading to higher ohmic loss. In addition to ohmic loss, transmission lines also have dielectric loss which also scales with frequency. In transmission lines, waves propagate as E(z) = E0e −(α+iβ)z, where α is the attenuation constant (not the loss parameter in RCM) given by α ≈ (ωε′′/2) √ µ/ε′ in which ε = ε′−jε′′ is the complex permittivity of the dielectric. So α ∝ ω and the wave decays much faster when frequency goes up. However, it is a challenge to properly collimate the free-space beam. For free- space propagation, the dielectric loss in air is negligible, and the reflection at the horn antenna due to the impedance mismatch is also very small, about -20 dB (1% of power is reflected). The only significant factor for losing signal strength is the im- perfect collimation. Since the frequency is not in the visible light spectrum range, it is not easy to properly position the antenna and lens to guarantee best collimation. But through careful experimentation, we can achieve an average transmission am- plitude of -5 dB across a 1 meter transmission distance for WR3.4 band (220 ∼ 330 GHz). For comparison, the loss of a 1 meter long gold-plated waveguide (about $1000 per 5 cm piece)would be 14 ∼ 20 dB, according to the Virginia Diode Inc waveguides data sheet [60]. 35 2.3.4 Mode Stirrer Since the RCM is a statistical theory, an ensemble of scattering systems is required to determine the system-specific features and the statistical properties of the en- closures. Consequently, we need to perturb the cavity modes while maintaining the volume of the cavity such that each measurement is a unique realization of the cavity with the same loss parameter. A typical method to create many realizations is to rotate a large metal panel inside the cavity (a “mode stirrer”), as used in Refs. [6, 23, 61, 62]. But for our setup, which has very high frequency and is sitting inside the cryostat in low temperature, we need to consider the following issues: • The motor that powers the panel must be able to work in high vacuum and low temperatures. The heat generated by the motor coil can quickly build up in vacuum with normal motors, and the motor material and design must be carefully chosen such that thermal contraction won’t cause mechanical prob- lems. • The cavity must be tightly enclosed by metal walls since any small gap or hole can leak out the electromagnetic waves reverberating inside. Normally The hole on the wall to host the panel axis is not a problem since the microwave wavelength (a few centimeter) is much larger than the hole diameter (a few millimeter). But with the wavelength scaled into the millimeter range, the leakage through the hole is substantial. To meet these requirements, we designed a magnetically coupled mode stirrer 36 powered by a cryogenic stepper motor, as shown in Figure 2.8. The cryogenic stepper motor (Phytron VSS 52.200.2.5UHVC) is suitable for ultra high vacuum (up to 10−11 mbar) and cryogenic temperature environment, typically used in space applications. The motor rotates a magnetic strip outside the cavity which is magnetically coupled to another magnetic strip inside the cavity, thus eliminating the need for an opening on the wall or direct mechanical contact. The metal mode-stirring panel is attached to the inside magnetic strip and rotates when the stepper motor rotates. It is worth noting that we do not need to control the exact location or the shape of the perturber for any given measurement, which would be an extremely difficult task in such a high frequency (and short wavelength) regime. The goal is to create an ensemble of scattering systems which differ in detail, but all have the same underlying statistical properties. Since the sole purpose of introducing the perturber is to scatter the waves in a different way without changing the statistical properties of the cavity (i.e. the loss parameter α) the precise location and orientation of the perturber is not important. However, it is important that we rotate and move the perturber to uniquely different orientations and positions, so that a diverse set of cavities with different scattering properties is created, enabling a high quality statistical ensemble. In experiments, the motor rotates a small step then waits for the Vector Net- work Analyser (VNA) to measure the S-parameters of the cavity in the current realization. When the VNA measurement is complete, the motor rotates again, and this process is repeated. Representative S-parameter measurements for two nearby realizations of the cavity and perturber are shown in Fig. 2.8 (b). In this way, data 37 for 200 highly uncorrelated realizations of the full-scale cavity is collected and used to obtain statistics of the electromagnetic properties, and to calculate the ensem- ble average required by the RCM to characterize system-specific properties. After collecting the ensemble S-parameter data, we check to see if each realization is sta- tistically independent to a significant degree from all the others by looking at their correlation coefficient. The Matlab function “corrcoef” is used for this purpose. We then construct the impedance matrix for the cavity data Zcav as described in Sec- tion 1.4. The ensemble averaged impedance is obtained as Zavg = 〈Zcav〉realizations for each measured frequency point. A histogram of the impedance values is constructed by taking the real or imaginary part of a matrix element of the Z-matrix over the entire ensemble (9 realizations for the miniature cavity or 200 realizations for the full-scale cavity) and over the whole frequency range (75 - 110 GHz for the miniature cavity or 3.7 - 5.5 GHz for the full-scale cavity). For the miniature cavity, since the cavity is gradually changing temperature, also changing the cavity loss, we can only measure 9 realizations in a half hour window before the loss between the first and last measurement differ significantly. It turns out that the large number of data points for many modes within the broad frequency bandwidth compensates the lack of realizations and we still get good statistics. 38 Figure 2.8: Magnetically coupled mode stirrer powered by a cryogenic stepper motor. The magnetic strip outside the cavity (lower yellow bar in the left side) is coupled by static magnetic field with the magnetic strip inside the cavity (upper yellow bar in the left side), eliminating the need for any hole on the wall. The upper right inset is an example of the mode stirrer placed inside the cavity. 39 2.4 Testing Experiments In a larger picture, our final goal is to test the RCM prediction of the statistics of the energy coupled into the N th cavity in a cascade of connected cavities using the setup introduced in Section 2.3. This work is in collaboration with U.S. Naval Research Laboratory (NRL). As a first step, our colleagues at NRL measured a full-scale 66 cm X 122.5 cm X 127.5 cm aluminum cavity at 3.7 ∼ 5.5 GHz (WR187 band) and 5.5 ∼ 8.25 GHz (WR137 band). We measured 2 scaled cavities with s = 20, scaling from 3.7 ∼ 5.5 GHz to 75 ∼ 110 GHz, and s = 40, scaling from 5.5 ∼ 8.25 GHz to 220 ∼ 330 GHz, respectively. After confirming that the scaled-down setup produces the same statistical impedance for the same α as the full-scale setup, we can proceed to investigate the statistical property of the connected cavities. In this section, we perform a series of experiments that can verify the operation of our experimental setup. Since the combination of the frequency extenders, remote injection and cryogenic environment was never explored before, we take progressive steps to study each component individually. Then later in section 4 we present the single cavity experiment result to confirm that the setup produce the same statistics, and in section 5 we discuss the multiple cavity experiment result. 2.4.1 Overall Plan Since this experimental setup is rather complex and has not been studied by any research group known to us, we take the following incremental steps towards the final goal making sure that we understand the results at each stage. 40 1. Obtain good transmission at mm-wave frequencies for the free-space propaga- tion path between two horn antennas. 2. Directly measure the scaled cavity, without the free-space propagation path, perturb the cavity modes using the magnetically coupled mode stirrer and repeat the measurements. Confirm that the collected realizations represent a good ensemble of the cavity. In all following experiments, a “measurement” means collecting an ensemble of data rather than measure the cavity at one single state. 3. Directly measure the scaled cavity, without the free-space propagation path, and calculate its loss parameter α at room temperature. This is called a “direct injection” measurement. 4. Measure the scaled single cavity at room temperature with the free-space propagation path installed and compare the calculated α with direct injection. This is called a “remote injection” measurement. 5. Put the remote injection setup in the cryostat to perform the same measure- ment at low temperatures. Note that this involves propagating the mm-wave signals through windows on each free-space path. We expect to see a de- crease of α with decreasing temperature. We compare the obtained α values to the result of the full-scale setup measurement done by our collaborators at NRL making sure that the scaled setup works well for a single cavity. This is discussed in section 4. 41 6. Extend the scaled single cavity setup to multiple connected cavities. Investi- gate the statistics of the power coupled into the N th cavity and test the RCM predictions in [3, 24]. This is discussed in section 5 The rest of the section 2.4 discuss items 1 to 4 on this list. 2.4.2 Free-space Propagation Path Measurement The purpose of this measurement is to determine the best distance between the antenna and the Teflon lens in order to get the optimal transmission through free- space. The two antennas are placed at a fixed distance, about 110 cm apart, and the lenses are placed at a distance of d1 from the transmitter horn antenna and d2 from the receiver horn antenna. All elements are aligned to be on a single line and only d1, d2 are varied. The average transmission is plotted in Figure 2.9 with the best values of d1, d2 enclosed in the yellow dotted circle. For the WR10 band, d1 = d2 = 10.45 cm and for the WR3.4 band, d1 = d2 = 15.45 cm. 2.4.3 Collecting an Ensemble of Cavity Data This experiment tests if the magnetically coupled mode stirrer can effectively per- turb the cavity modes in the cryogenic environment. An example of the measured reflection (S11) and transmission (S21) magnitude data for the s = 20 cavity is plot- ted in Figure 2.10 for 5 realizations. Notice that the full frequency range plot for |S11| on the top left shows that all curves follow the slowly varying trend which is the non-statistical system specific feature, while the zoom-in plot on the top right 42 Figure 2.9: The transmission amplitude in dB for free-space propagation measure- ment. The x-axis and y-axis are the distance between the lens to the transmitter antenna (d1) and the receiver antenna (d2) respectively. The yellow dotted circles enclose the region for best d1, d2 values for optimal transmission. shows that each curve differs dramatically from each other, which is the result of the mode stirrer perturbing the cavity modes. It is clear from Figure 2.10 that the cavity modes are indeed perturbed but we need to further ensure that realizations are uncorrelated with each other and represent a statistically sound ensemble. To do this, we adopt the use of the power ratio Λ defined in Ref. [2] as the ratio of the maximum transmitted power to the minimum transmitted power at each frequency for all mode stirrer positions, i.e. Λ = max(|S21|2)/min(|S21|2). Λ is a function of frequency and should have a large mean and a large dynamic range if the cavity modes are well perturbed and uncorrelated, which gives us a good ensemble of data. To see how Λ distinguishes a good ensemble from a bad one, we plot two Λ spectra calculated from 2 ensembles, each consisting of 9 realizations, and their histograms in Figure 2.11. The Λ in the left figure, which represent a good ensemble, has a mean of about 15 dB and a dynamic range of 40 dB, 43 Figure 2.10: Experimentally measured reflection (top two plots) and transmission (bottom two plots) magnitude for the s = 20 cavity for 5 realizations created by rotating the magnetically coupled mode stirrer. The left column plots the data in the full frequency range from 75 GHz to 110 GHz while the right column zooms in a 100 MHz window. Each curve is wildly different from others but yet follow the same slowly varying trend which is the non-statistical system specific feature. 44 Figure 2.11: Power ratio Λ as a function of frequency and its histogram for a good ensemble (left) and a bad ensemble (right) data. Λ should have a large mean and a large dynamic range if the cavity modes are well perturbed and uncorrelated, which gives us a good ensemble of data. indicating large field fluctuations as the mode stirrer rotates. On the contrary, the Λ on the right figure has an almost zero mean and 15 dB dynamic range, suggesting high correlation between realizations. In fact, the data in the right figure were taken when the mode stirrer was stuck and not moving. 2.4.4 Direct Injection The purpose of the direct injection experiment is to get an accurate value for the cav- ity loss parameter α before applying conductivity scaling and without the influence of the free-space propagation path. As shown in Equation (2.2) if we only scale the cavity size and measurement frequency, then the loss parameter α ∝ √ s/σ. Based on the previous RCM ex- periment on the full-scale cavity [6], α(s = 1) ≈ 2.05 for 3.7 ∼ 5.5 GHz and α(s = 1) ≈ 5.95 for 5.5 ∼ 8.25 GHz as shown in Figure 2.12. Thus we are expecting 45 Figure 2.12: Loss parameter α values for the full scale cavity measured by col- laborators at U.S. Naval Research Laboratory. Each α value is calculated from experimental data in a 0.1 GHz window at the specified frequency. The data points are taken from Table 1 in [6]. α(s = 20) ≈ √ 20α(s = 1) = 9.17 for the WR10 band and α(s = 40) ≈ √ 40α(s = 1) = 37.6 for the WR3.4 band. As mentioned in Section 2.2.2, the scaled cavity ma- terial is copper (and the full-scale cavity material is aluminum) so there is a scaling up of conductivity √ σCu/σAl = √ 5.96/3.50 = 1.30. Thus the α we should see for the s = 20 (WR10 band) cavity is 9.17/1.30 = 7.05, and for the s = 40 (WR3.4 band) cavity is 37.6/1.30 = 28.9. Notice that these are just estimates, based on the metal bulk conductivities for pure metal. In experiments, the actual ohmic loss depends on the surface resistance and the penetration depth, which is influenced by the impurity, surface roughness [58, 59], temperature and is frequency-dependent. The PDF of the normalized impedance for a direct injection experiment on a scaled-down s = 20 copper cavity is shown in figure 2.13. By fitting with the RCM predictions for the PDF for various α, which is obtained through a series of Monte Carlo simulations with different α values, we determined that α = 4.5 for the direct 46 Figure 2.13: Probability Density Function (PDF) of the normalized impedance for a direct injection experiment on a scaled-down s = 20 copper cavity (dotted line), in comparison with the RCM Monte Carlo simulation with α = 4.5 (solid line). injection setup. This value is close to what we expect, which is about 7. It was later discovered from the time-domain method, discussed in section 3.2.2, that this α = 4.5 is actually an overall α that includes both the cavity’s loss and the loss in the short waveguide section in the cavity wall. The copper cavity has a quarter inch thick wall and the mm-wave enters and exits the cavity through two rectangular openings on the wall, which are essentially two quarter inch long waveguides. The waveguides in the wall add up the total loss and need to be excluded from the total loss, characterized by α = 4.5 in the direct injection experiment, to reveal the true cavity loss. This is done by introducing the radiation efficiency η into the RCM, which is discussed in chapter 3. 47 2.4.5 Remote Injection The remote injection measurement is similar to the direct injection except that the two free-space propagation paths, one at the transmitter end and one at the receiver end, must be installed, as shown in Figure 2.7. The α value calculated from Equation 1.4 is around 30, much higher than the direct injection α value because of the influence from the lossy free-space propagation path. The RCM normalization procedure in Section 1.5 can only normalize out the system-specific features that are lossless. Without any modification to Equation 1.4, the obtained α represent the overall lossyness, including the cavity and the lossy free-space path. If we consider the lossy free-space path together with the horn antennas as a complex “port” or a composite “antenna”, then this can be generalized into the problem of RCM with lossy ports. The solution is to use the radiation efficiency to quantify the lossyness of the ports and then properly exclude it from the overall α. This is discussed in detail in Chapter 3. 2.4.6 Extension to Multiple Connected Cavities The experimental setup and the results for multiple scaled cavities are discussed mainly in Chapter 5. As a brief preview, the life-size 3D-printed model of the system and the configuration for a 3-cavity cascade is shown in Figure 2.14. This design is for s = 20 and has the advantage of being reconfigurable, extendable and is compatible the remote injection setup in the cryostat. The backplane is a thin metallic plate, which is vertically attached to the cold 48 Figure 2.14: 3D-printed model of the multiple connected cavities and the configu- ration for a 3-cavity cascade drawn in CST. plate in the cryostat, and has screw holes for mounting the rectangular cavities. It also has apertures to couple the cavities mounted on one side to the ones mounted on the other side. If we view the backplane as a grid, where each grid cell has a circular aperture at its center, then the cavity is a 2-cell block having 5 walls. And once mounted to the backplane, it will have 2 open apertures. There are two special cavities that have a rectangular opening on the side, as highlighted in Figure 2.14 as ”ports”. The rectangular opening is covered by a special adapter that has the Teflon lens attached to it, positioned at a certain distance to the antenna and is well aligned. The three blocks attached to the backplane in Figure 2.14 is an example of a simple 3-cavity cascade. In the left figure, the 2 gray cavities at the front are the first and third cavity which will have the horn antennas installed on the rectangular apertures. They both couple to the green cavity on the other side through large circular apertures on the backplane. The 3-cavity cascade model is also shown in Figure 2.15 with cavity walls and backplane omitted. With this grid-cell model we can easily compose any N -cavity cascade and 49 Figure 2.15: The air region of the 3-cavity cascade model with cavity walls and backplane omitted. The wave goes into the first cavity through the antenna mount- ing point, then couples into the second cavity mounted on the other side of the backplane (not shown) through an aperture. It is then coupled to the third cavity through the other aperture, and gets out through the antenna mounting point on the third cavity. place it in the remote injection setup to measure its characteristics. For this s = 20 scaled cavity size, we can easily put 20 cavities on each side of the backplane, more than enough for the connected cavity analysis. Furthermore, we can put additional backplanes parallel to the existing one to host additional cavities. This design allows us to investigate many interesting coupled cavity configurations beyond the theory prediction. 2.4.7 Further Studies The remote injection scaled measurement setup described in Section 2.3 combined with the grid-cell cavity design mentioned above opens up the opportunity to study RCM predictions in a network of connected cavities. In the grid-cell cavity design, cavities are basically 2-cell blocks and thus are 50 2-port cavities with the apertures acting as the port connecting to other cavities. We can extend the cavities to be 3-cell or 4-cell blocks that covers 1X3 cells or 2X2 cells making them 3-port or 4-port cavities. Their volume can be maintained by changing the height of the cavities. If we consider the cavities as nodes, we can arrange them on the backplane such that they form a network, such as a tetrahedron (3-branch nodes) or a pentagon (4-branch nodes). The linear cascade that we are going to study initially is the case of the simplest network, as illustrated in Figure 2.16. By changing the cavities from 1X2 blocks to 2X2 blocks, we can use the similar setup to study complicated graphs as shown in Figure 2.17. The example network has a total of seven connected scaled cavities that are of difference sizes and have anywhere from one to four apertures. Each cavity is represented as a node and each aperture is represented as an edge in the graph. Limited only by the size of the cryostat interior, the number of different networks that we could study with this experimental setup is orders of magnitude larger than that with a conventional full scale cavity setup. Furthermore, the volume inside the cryostat is so large compared to the scaled- down cavities that we can potentially shrink even larger structures. For example, the cryostat’s cylindrical space of diameter d = 50 cm and height h = 50 cm is equivalent to a full scale cylinder of